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1、SPEX SamplePrepEquipment Lineup,Product Lines,Freezer/MillGeno/GrinderPressesMixer/MillShatterboxXRF accessories,Freezer/Mills,67706870,What is Cryogenic Grinding?,The Ultimate Sample Preparation Technique for Pulverizing“Difficult”SamplesGrinding materials at low temperatures.Liquid Nitrogen 196C,W
2、hy Cryogenic Grinding?,Have difficult samples to prepare?You tried every technique in your laboratory and nothing works?Feel that nothing in this world will grind your samples?,Advantages:,“Ungrindable”samples can be pulverizedLeaves,roots,stems,seeds(cotton,sunflower,corn)Polymers,rubber,siliconesF
3、ibers,hair,textilesSkin,bone,muscle,cartilage,etcFood products,paint chips,pharmaceuticalsGums,resins,waxesElectronic componentsTough food,feed materials(dog chews),Before&After,Leather,Corn,Bone,A Collection of our Before&After Samples,6770/6870Freezer/Mill(Biotechnology)&Numerous other application
4、s,Spex SamplePrep freezer mills are the only true“Cryogenic Mills”on the market for over 40 years.Utilized for grinding fresh plant and animal tissue for nucleic acids(RNA/DNA),forensics,GMO analysis and genetic researchUseful tool for pharmaceutical analysis,drug testing,medical research,polymers a
5、nd plastics.RoHs/WEEE testing,6770/6870 Freezer/Mill:Features&Benefits,Cryogenic mills which chill samples to liquid nitrogen temperatures(-196C)Magnetically driven impactor is the only moving partNo mechanical linkages or bearings to failGrinding vials are sealed so sample integrity is maintained d
6、uring grinding cycleEquip with speed control,programmable timer,and safety interlock.Sample sizes from 0.1g to 50g,6770/6870 Freezer/Mill:Features&Benefits,Integral LN reservoir maintains cryogenic temperaturesProgrammable LCD Touch Screen ControlsMultiple User Memory SettingsThe only mill to grind
7、samples in LN.This ensures optimum sample brittleness for best resultsHas integral pre-cooling positions(reduced LN consumption,safe storage of ground samples,no external chilling equipment needed)Auto-fill option(6870 only)-time saving and increased safetyLow cost vials with easy sample extraction-
8、important for forensic and pharma customers who need disposable vialsSeveral vial options,micro vials,regular,mid size and large,Applications/where to sell,Forensic Labs DNA identificationMedical Laboratories genetic research,disease preventionHospital Labs For genetic screening(oncology,etc)Agricul
9、tural Labs For crop development and GM testingAgricultural Veterinary Labs For livestock breeding and healthArchaeology Labs Ancient DNA ExtractionPublic Health and Environmental Monitoring LaboratoriesContract/commercial testing labs QC of manufactured goodsElectronics Companies grinding electronic
10、 components,Freezer mills 6770&6870Applications and Markets,Other new markets and opportunitiesElectronics companies-grinding soft metals(Aluminium,Zinc)Pharmaceutical companies grinding capsules and whole tabletsDentistry-grinding amalgams,resinsFood safety toxicity testingPhthalates in plastics-ne
11、w regulations,New CPSC Guidelines for Determination of Phthalates in Plastics,Consumer Product Safety Commission(CPSC)standard operating procedure for determining phthalates in plastics in childrens toysOperating procedure recommends the use of cryogenic grinding to prepare samplesCryogenic grinding
12、 can pulverize samples down to a fine powder of less than 500 micronsCreates homogenous sample with a larger surface area improving the extraction process.,Freezer/Mill in Action,6770 in CSI Miami(Season 7 Ep.2),Used in studies of Moon Rock,Geno/Grinder,2010,2010 Geno/Grinder(Biotechnology),The 2010
13、 Geno Grinder was specifically designed for Pioneer Hybrid International“A World Leader in genetic crop science”.The Geno/Grinder provides a mechanism for efficient cell disruption of plant and animal tissue for the isolation of nucleic acids(RNA/DNA),enzymes,yeast and proteins.The versatile sample
14、clamping mechanism can also hold micro-tubes,racked tubes,specially designed 5 ml vials,15ml and 50 ml standard conical tubes using the optional large capacity clamp adapter.,2010 Geno/Grinder:Features&Benefits,Unique true vertical action ensures complete sample processing.Sample clamp accepts multi
15、ple micro titer-plates,various vials from 0.6ml to 50ml vials-wide application range.Adjustable speed control and timer(with countdown display)for optimum results.Wide range of cryogenic accessoriesWide range of grinding media,NEW FEATURESModern,streamlined lookSmaller footprintLighterLCD DisplayImp
16、roved reliability of wear parts,2010 Geno/Grinder:Accessories,Cryo-Station A holding station for temperature sensitive samples such as proteins and pesticidesCryo-Adapter A single piece of extruded aluminium to be chilled and then inserted into a 2210 96-well Titer PlateCryoBlocksAluminium blocks de
17、signed to hold samples for chilling in the Cryo-station.Cryo-Blocks come in a variety of holding sizes including 0.6 mL&2.0 mL PCR tube capacity.CryovialsPC and PE centrifuge tubes specifically designed to resist breaking at low temperatures.Ideal for grinding temperature sensitive samples.,Kryo-Tec
18、h accessories,2000 Geno/Grinder Applications,Rapid preparation of multiple samples for PCR samplingFast disruption to allow extraction of Nucleic acidsHigh-throughput in a 96-well format and various other formats up to twelve 50mL centrifuge tubesLysing of bacterial cellsDNA screening for disease co
19、ntrolPesticide analysis,2010 Geno/Grinder,Where to Sell,Basically any institution using high throughput DNA sample processingPlant and Animal development companies Agricultural and public health labs(disease screening).Pesticide residuesMicro toxins,Markets,Look for synergy!-DNA sequencing equipment
20、,Cell washing equipment,Microplate sealing equipment.,2010 Geno/Grinder,QuEChERS Method,QuickEasyCheapEffectiveRuggedSafe,Plant tissue from Fruits and Vegetables are homogenized and mixed with QuEChERS reagents using Geno/Grinder&ceramic grinding mediaCan be homogenized at room temperature or with K
21、ryo-Tech accessoriesUp to 16 x 50ml vials can be processed simultaneouslyIncreases pesticide yieldsImproves reproducibilityUsed by FDA,Geno/Grinder Sales Focus,Primarily high-throughput usersCapital costs are easily countered by time savingsMultiple sample format flexibilityAppeals to a broad spectr
22、um of users and applicationsPedigree of existing usersName drop use the reference list to its full benefitProfile of existing usersLook for similarities between current and potential users,Example Customers:Danish Institute of Agricultural Science|Planta,GermanyPioneer,France|Monsanto,UK|Syngenta,UK
23、Rijk Zwaan,Netherlands|Enza Zaden,NetherlandsPioneer Hybrid,USA|Du Pont,USA|Promega,USAUS Dept.of Agriculture|Aventis Crop Science,USA|Merck,USA,X-Press&Bench-Press,3635/3628,Presses,3635 X-Press,New anodized look with the same rugged reliability The X-Press is a 35 ton fully automated hydraulic pre
24、ss used for spectroscopic techniques requiring samples in the form of round,flat-surfaced discs,most commonly XRFSPEX SamplePrep presses and dies are sophisticated in design,but functionally simple and provide years of maintenance-free operation.,New!,Now featuring a programmable LCD touch screen Fu
25、lly Programmable-Final pressure desired,time to hold at final pressure,and intervals to return back to zero pressureTypical pressing cycle is less than two minutesA safety interlock and automatic pump shut-off safety valve ensure safe operationCompact,bench top operationAccepts all competitors die s
26、etsCE marked,3635 X-Press,Features and Benefits,3628 Bench-Press,The 3628 Bench-Press is an air-actuated,manually controlled 25-ton laboratory press.This Bench-Press is compact Very simple controlsIt includes a safety door with interlock,CE-markedAccepts most other“stand-alone”pellet dies.Good for s
27、park free environments,Users of XRF instrumentsUniversities notably Geology Depts.Cement manufacturingAny industrial facility requiring analysis or processing pelletized samplesMarkets and customers similar to Shatterbox and Mixer mills Look for Synergy!(work with XRF supplier offices/sales reps in
28、your regions),X-Press&3628,Where to Sell,Mixer/Mill,51008000M8000D,Pulverizing&Blending,Can hold up to 3 small vials,20 g sample using two vials,Efficient laboratory mill for pulverizing hard,brittle samples Often described as a shaker mill or high-energy ball millCapable of rapidly reducing solids
29、to analytical fineness or blending a wide range of powdersEffective for mechanical alloying,well documented in literature“SPEX Mill”Extended run timesMembrane control panel Built in Fan for cooling,8000M Mixer/Mill,Features&Benefits,Mixer/Mills,Mixer/Mill is only ball mill that can be used for effic
30、ient Mechanical alloying.Figure of Eight motion has been proven to be more efficient than side-to-side or planetary motion found in other millsExtremely robustLarge range of grinding vial materials and size Competitively priced,Universities,geology,materials science,engineering departmentsIndustrial
31、 laboratories-cement,slag,ceramics,catalystsPharmaceutical companies(Blending,polymers)Rock LabsElectronics(mechanical alloying)Petroleum companiesCorn milling method G-11 Hexane extraction methodhttp:/corn.org/methods/G-11.pdf,Mixer/Mills,Where to Sell,Shatterbox,8530,Shatterbox 8530,The Shatterbox
32、 is the most popular“swing mill”in AmericaIt is the most efficient way to grind brittle samples to analytical finenessThe Shatterbox swings a dish-shaped grinding container with a puck and ring,in a tight high-speed circle Fast grinding times,Resultant particle size well below 200 mesh;with proper g
33、rinding aid,less then 10 micronsWide choice of grinding container material and sizeClamp requires only moderate hand pressure to secure grinding dish and is adjustable to secure containers of different heightsVial transporter availableSoundproof enclosure,variable-range electronic timer,lockable cas
34、ters&safety interlock systemMembrane control panel resistant to airborne particles,Shatterbox 8530,Features&Benefits,Shatterbox 8530,Same markets as mixer/millsNotably mining operations(prefer larger samples sizes)Pharmaceuticals,dried marsh grass,and many other materials,Where to Sell,Spec-Caps Sha
35、llow,thin-walled aluminum cups routinely used to produce pressed-powder sample discs for XRF.Sizes available for all die sets.X-Cells for XRF Liquid SamplesPatented closed X-Cell design prevents spillage in inverted XRF spectrometers.Sizes to fit most instruments.Thin Film Windows for XRF Necessity
36、for X-Cell liquid sample cell,serving as a the sample window.Different types available based on sample characteristics.Eg Mylar,XRF Accessories,Provide a high profit margin and continuous revenue streamLet users have samples we can provide sample packs for trial with key potential usersLook for synergy with XRF instrument manufacturers&suppliersBulk quantities available for lower price,XRF Accessories,Features&Benefits,Thanks for your attention,
